Information card for entry 7026791

Structure parameters

• Chemical name: N,N-bis-dichlorophosphino-2,6-bis-(2,4,6-trimethylphenyl)aniline
• Formula: C24 H25 Cl4 N P2
• Calculated formula: C24 H25 Cl4 N P2
• SMILES: P(Cl)(Cl)N(P(Cl)Cl)c1c(cccc1c1c(cc(cc1C)C)C)c1c(cc(cc1C)C)C
• Title of publication: Synthesis of sterically encumbered 2,4-bis-m-terphenyl-1,3-dichloro-2,4-cyclo-dipnictadiazanes [m-TerNPnCl](2), (Pn = P, As).
• Authors of publication: Reiss, Fabian; Schulz, Axel; Villinger, Alexander; Weding, Nico
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2010
• Journal volume: 39
• Journal issue: 41
• Pages of publication: 9962 - 9972
• a: 16.571 ± 0.003 Å
• b: 17.535 ± 0.004 Å
• c: 17.726 ± 0.004 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 5150.7 ± 1.9 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.071
• Residual factor for significantly intense reflections: 0.0441
• Weighted residual factors for significantly intense reflections: 0.1151
• Weighted residual factors for all reflections included in the refinement: 0.1265
• Goodness-of-fit parameter for all reflections included in the refinement: 1.061
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No