Information card for entry 7026793

Structure parameters

• Chemical name: N,N',N'-[Tris-(trimethylsilyl)]hydrazino- [2,6-bis-(2,4,6-(trimethylphenyl)phenyl]imino-phosphane
• Formula: C33 H52 N3 P Si3
• Calculated formula: C33 H52 N3 P Si3
• SMILES: P(=Nc1c(cccc1c1c(cc(cc1C)C)C)c1c(cc(cc1C)C)C)N([Si](C)(C)C)N([Si](C)(C)C)[Si](C)(C)C
• Title of publication: Synthesis of sterically encumbered 2,4-bis-m-terphenyl-1,3-dichloro-2,4-cyclo-dipnictadiazanes [m-TerNPnCl](2), (Pn = P, As).
• Authors of publication: Reiss, Fabian; Schulz, Axel; Villinger, Alexander; Weding, Nico
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2010
• Journal volume: 39
• Journal issue: 41
• Pages of publication: 9962 - 9972
• a: 10.684 ± 0.002 Å
• b: 11.033 ± 0.002 Å
• c: 16.094 ± 0.003 Å
• α: 86.43 ± 0.03°
• β: 82.08 ± 0.03°
• γ: 75.71 ± 0.03°
• Cell volume: 1820.1 ± 0.6 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0608
• Residual factor for significantly intense reflections: 0.0426
• Weighted residual factors for significantly intense reflections: 0.1117
• Weighted residual factors for all reflections included in the refinement: 0.1193
• Goodness-of-fit parameter for all reflections included in the refinement: 1.064
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No