Information card for entry 7027050

Structure parameters

• Formula: C42 H59 B N5 O4 Tc
• Calculated formula: C42 H59 B N5 O4 Tc
• Title of publication: Crystal structures of nitridotechnetium(V) complexes of amine oximes differing in carbon chain lengths
• Authors of publication: Kani, Yuko; TakayamaTsutomuSekine, Tsutomu; Kudo, Hiroshi
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 1999
• Journal issue: 2
• Pages of publication: 209
• a: 9.986 ± 0.005 Å
• b: 30.636 ± 0.002 Å
• c: 13.967 ± 0.003 Å
• α: 90°
• β: 95.24 ± 0.03°
• γ: 90°
• Cell volume: 4255 ± 2 ų
• Cell temperature: 286.2 K
• Ambient diffraction temperature: 286.2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for significantly intense reflections: 0.0337
• Weighted residual factors for significantly intense reflections: 0.036
• Goodness-of-fit parameter for significantly intense reflections: 1.3
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No