Information card for entry 7027088

Structure parameters

• Formula: C21 H41 Cl3 N4 Nb2 S9 Te2
• Calculated formula: C21 H41 Cl3 N4 Nb2 S9 Te2
• Title of publication: Substitution of bridging S2 ligands in the [Nb2(μ-S2)2]4+ core: a simple route to [Nb2(Se2)2]4+, [Nb2(S)(Te2)]4+ and [Nb2(S)2]4+
• Authors of publication: Sokolov, Maxim; Imoto, Hideo; Saito, Taro; Fedorov, Vladimir
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 1999
• Journal issue: 1
• Pages of publication: 85
• a: 13.03 ± 0.003 Å
• b: 14.391 ± 0.005 Å
• c: 12.053 ± 0.004 Å
• α: 97.61 ± 0.03°
• β: 110.81 ± 0.02°
• γ: 78.4 ± 0.03°
• Cell volume: 2064.9 ± 1.2 ų
• Cell temperature: 173.2 K
• Ambient diffraction temperature: 173.2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for significantly intense reflections: 0.091
• Weighted residual factors for significantly intense reflections: 0.0554
• Goodness-of-fit parameter for significantly intense reflections: 2.568
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No