Information card for entry 7027101

Structure parameters

• Formula: C46 H51 B Cl N7 O4 Pb
• Calculated formula: C46 H51 B Cl N7 O4 Pb
• Title of publication: Lead complexation by novel phenanthroline-containing macrocycles †
• Authors of publication: Bazzicalupi, Carla; Bencini, Andrea; Fusi, Vieri; Giorgi, Claudia; Paoletti, Piero; Valtancoli, Barbara
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 1999
• Journal issue: 3
• Pages of publication: 393
• a: 9.777 ± 0.007 Å
• b: 13.7 ± 0.01 Å
• c: 16.75 ± 0.01 Å
• α: 89.16 ± 0.07°
• β: 84.9 ± 0.1°
• γ: 71.9 ± 0.1°
• Cell volume: 2124 ± 3 ų
• Cell temperature: 298 K
• Ambient diffraction temperature: 298 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.191
• Residual factor for significantly intense reflections: 0.1031
• Weighted residual factors for all reflections: 0.3231
• Weighted residual factors for significantly intense reflections: 0.2519
• Goodness-of-fit parameter for all reflections: 1.026
• Goodness-of-fit parameter for significantly intense reflections: 1.142
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No