Information card for entry 7027103

Structure parameters

• Formula: C32 H62 K2 O3 Si3
• Calculated formula: C32 H62 K2 O3 Si3
• SMILES: [K]([O]1CCCC1)[O]1CCCC1.[K][O]1CCCC1.[Si](C)(C)(C)[C-]1C=C(CCC1)[Si](C)(C)C1=C[C-](CCC1)[Si](C)(C)C
• Title of publication: Synthesis and structures of some silylallyl-lithium or -potassium complexes
• Authors of publication: Hitchcock, Peter B.; Lappert, Michael F.; Leung, Wing-Por; Liu, Dian-Sheng; Mak, Thomas C. W.; Wang, Zhong-Xia
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 1999
• Journal issue: 8
• Pages of publication: 1257
• a: 17.298 ± 0.001 Å
• b: 20.032 ± 0.001 Å
• c: 11.727 ± 0.001 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 4063.6 ± 0.5 ų
• Cell temperature: 294 ± 2 K
• Ambient diffraction temperature: 294 ± 2 K
• Number of distinct elements: 5
• Space group number: 33
• Hermann-Mauguin space group symbol: P n a 21
• Hall space group symbol: P 2c -2n
• Residual factor for all reflections: 0.108
• Residual factor for significantly intense reflections: 0.0989
• Weighted residual factors for significantly intense reflections: 0.2606
• Weighted residual factors for all reflections included in the refinement: 0.2684
• Goodness-of-fit parameter for all reflections included in the refinement: 1.148
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No