Information card for entry 7027123

Structure parameters

• Formula: C20 H28 Cl N4 P2 Sb
• Calculated formula: C20 H28 Cl N4 P2 Sb
• SMILES: [Sb]12(Cl)[N]3(P(N(C(C)(C)C)P3N2c2ccccc2)N1c1ccccc1)C(C)(C)C
• Title of publication: Polycyclic bis(amido)cyclodiphosphazane complexes of antimony(III) and bismuth(III): syntheses, molecular structures and solution behaviour
• Authors of publication: Moser, Daniel F.; Schranz, Ingo; Gerrety, Michael C.; Stahl, Lothar; Staples, Richard J.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 1999
• Journal issue: 5
• Pages of publication: 751
• a: 11.0596 ± 0.0002 Å
• b: 24.5139 ± 0.0002 Å
• c: 18.1872 ± 0.0003 Å
• α: 90°
• β: 98.396 ± 0.001°
• γ: 90°
• Cell volume: 4877.96 ± 0.13 ų
• Cell temperature: 213 ± 2 K
• Ambient diffraction temperature: 213 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0418
• Residual factor for significantly intense reflections: 0.0288
• Weighted residual factors for significantly intense reflections: 0.0655
• Weighted residual factors for all reflections included in the refinement: 0.0672
• Goodness-of-fit parameter for all reflections included in the refinement: 1.016
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No