Information card for entry 7027150

Structure parameters

• Formula: C24 H66 Cl17 Cu17 N6 O0 S6
• Calculated formula: C24 H66 Cl17 Cu17 N6 S6
• Title of publication: Self-assembling copper(I) clusters involving electron-deficient, quadruply bridging thiolate ligands
• Authors of publication: Prichard, Robin G.; Parish, R. V.; Salehi, Zahra
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 1999
• Journal issue: 2
• Pages of publication: 243
• a: 13.058 ± 0.004 Å
• b: 36.961 ± 0.006 Å
• c: 13.417 ± 0.002 Å
• α: 90°
• β: 92.54 ± 0.03°
• γ: 90°
• Cell volume: 6469 ± 2 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.2372
• Residual factor for significantly intense reflections: 0.1052
• Weighted residual factors for significantly intense reflections: 0.157
• Weighted residual factors for all reflections included in the refinement: 0.2101
• Goodness-of-fit parameter for all reflections included in the refinement: 1.26
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No