Crystallography Open Database

Information card for entry 7027154

Preview

Coordinates	7027154.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C51 H72 B Cl4 F4 N2 P2 Pt Rh
Calculated formula	C51 H72 B Cl4 F4 N2 P2 Pt Rh
Title of publication	A facile method for the synthesis of heterobimetallic chloro-bridged complexes containing (R3P)2MCl (M = Pt or Pd) fragments
Authors of publication	Polborn, Kurt; Severin, Kay
Journal of publication	Journal of the Chemical Society, Dalton Transactions
Year of publication	1999
Journal issue	5
Pages of publication	759
a	13.072 ± 0.002 Å
b	15.041 ± 0.002 Å
c	15.622 ± 0.003 Å
α	103.631 ± 0.013°
β	93.331 ± 0.015°
γ	103.126 ± 0.013°
Cell volume	2886.7 ± 0.8 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	9
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0365
Residual factor for significantly intense reflections	0.0304
Weighted residual factors for all reflections	0.0859
Weighted residual factors for significantly intense reflections	0.0805
Goodness-of-fit parameter for all reflections	1.101
Goodness-of-fit parameter for significantly intense reflections	1.099
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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