Co-ordination chemistry of CuI with 1,3,5-tris[bis(pyridin-2-ylmethyl)aminomethyl]-2,4,6-triethylbenzene, a conformationally constrained trinucleating ligand
Authors of publication
Walsdorff, Christian; Park, Sunyoung; Kim, Jeongho; Heo, Jungseok; Park, Ki-Min; Oh, Jinho; Kim, Kimoon
Journal of publication
Journal of the Chemical Society, Dalton Transactions
Year of publication
1999
Journal issue
6
Pages of publication
923
a
13.737 ± 0.0003 Å
b
14.5407 ± 0.0003 Å
c
16.7511 ± 0.0003 Å
α
65.871 ± 0.001°
β
83.257 ± 0.001°
γ
88.697 ± 0.001°
Cell volume
3031.31 ± 0.11 Å3
Cell temperature
188 ± 2 K
Ambient diffraction temperature
188 ± 2 K
Number of distinct elements
6
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.0698
Residual factor for significantly intense reflections
0.0529
Weighted residual factors for significantly intense reflections
0.12
Weighted residual factors for all reflections included in the refinement
0.1335
Goodness-of-fit parameter for all reflections included in the refinement
