Co-ordination chemistry of CuI with 1,3,5-tris[bis(pyridin-2-ylmethyl)aminomethyl]-2,4,6-triethylbenzene, a conformationally constrained trinucleating ligand
Authors of publication
Walsdorff, Christian; Park, Sunyoung; Kim, Jeongho; Heo, Jungseok; Park, Ki-Min; Oh, Jinho; Kim, Kimoon
Journal of publication
Journal of the Chemical Society, Dalton Transactions
Year of publication
1999
Journal issue
6
Pages of publication
923
a
16.5648 ± 0.0011 Å
b
16.5648 ± 0.0011 Å
c
5.3351 ± 0.0004 Å
α
90°
β
90°
γ
120°
Cell volume
1267.78 ± 0.15 Å3
Cell temperature
296 ± 2 K
Ambient diffraction temperature
296 ± 2 K
Number of distinct elements
3
Space group number
146
Hermann-Mauguin space group symbol
R 3 :H
Hall space group symbol
R 3
Residual factor for all reflections
0.029
Residual factor for significantly intense reflections
0.0282
Weighted residual factors for significantly intense reflections
0.0678
Weighted residual factors for all reflections included in the refinement
0.0689
Goodness-of-fit parameter for all reflections included in the refinement
