Information card for entry 7027227

Structure parameters

• Formula: C46 H32 Fe3 N8 O12
• Calculated formula: C46 H32 Fe3 N8 O12
• Title of publication: Syntheses, crystal structures and magnetic properties of two novel layered compounds: [Fe3(C2O4)3(4,4′-bpy)4] and [Co(C2O4)(4,4′-bpy)] (4,4′-bpy = 4,4′-bipyridine) †
• Authors of publication: Zheng, Li-Min; Fang, Xia; Lii, Kwang-Hwa; Song, Hui-Hua; Xin, Xin-Quan; Fun, Hoong-Kun; Chinnakali, Kandasamy; Razak, Ibrahim Abdul
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 1999
• Journal issue: 14
• Pages of publication: 2311
• a: 16.2475 ± 0.0002 Å
• b: 15.984 ± 0.0002 Å
• c: 16.3856 ± 0.0001 Å
• α: 90°
• β: 94.2776 ± 0.0003°
• γ: 90°
• Cell volume: 4243.49 ± 0.08 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1113
• Residual factor for significantly intense reflections: 0.0493
• Weighted residual factors for all reflections: 0.1127
• Weighted residual factors for significantly intense reflections: 0.0887
• Goodness-of-fit parameter for all reflections: 1.023
• Goodness-of-fit parameter for significantly intense reflections: 1.073
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No