Information card for entry 7027237

Structure parameters

• Formula: C88.61 H77.54 B2 Cl1.38 O4 P6 Pt2
• Calculated formula: C88.614 H77.535 B2 Cl1.386 O4 P6 Pt2
• Title of publication: Phosphine exchange reactions involving cis-[Pt(PPh3)2(Bcat)2] (cat = 1,2-O2C6H4) and the oxidative addition of 1,2-B2Cl2(NMe2)2 to Pt0
• Authors of publication: Curtis, David; Lesley, M. J. Gerald; Norman, Nicholas C.; Orpen, A. Guy; Starbuck, Jonathan
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 1999
• Journal issue: 10
• Pages of publication: 1687
• a: 22.88 ± 0.004 Å
• b: 14.21 ± 0.002 Å
• c: 26.731 ± 0.004 Å
• α: 90°
• β: 114.248 ± 0.01°
• γ: 90°
• Cell volume: 7924 ± 2 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1267
• Residual factor for significantly intense reflections: 0.0656
• Weighted residual factors for all reflections: 0.1418
• Weighted residual factors for significantly intense reflections: 0.1171
• Goodness-of-fit parameter for all reflections: 1.065
• Goodness-of-fit parameter for significantly intense reflections: 1.152
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No