Information card for entry 7027240

Structure parameters

• Formula: C38 H36 B Cl2 N P2 Pt
• Calculated formula: C38 H36 B Cl2 N P2 Pt
• Title of publication: Phosphine exchange reactions involving cis-[Pt(PPh3)2(Bcat)2] (cat = 1,2-O2C6H4) and the oxidative addition of 1,2-B2Cl2(NMe2)2 to Pt0
• Authors of publication: Curtis, David; Lesley, M. J. Gerald; Norman, Nicholas C.; Orpen, A. Guy; Starbuck, Jonathan
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 1999
• Journal issue: 10
• Pages of publication: 1687
• a: 10.865 ± 0.005 Å
• b: 12.093 ± 0.006 Å
• c: 14.228 ± 0.005 Å
• α: 95.819 ± 0.006°
• β: 92.523 ± 0.01°
• γ: 105.637 ± 0.006°
• Cell volume: 1786 ± 1.4 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0418
• Residual factor for significantly intense reflections: 0.0307
• Weighted residual factors for all reflections: 0.0616
• Weighted residual factors for significantly intense reflections: 0.0585
• Goodness-of-fit parameter for all reflections: 1.004
• Goodness-of-fit parameter for significantly intense reflections: 1.047
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No