Information card for entry 7027244

Structure parameters

• Formula: C44.6 H45.2 Cl1.2 N8 Yb
• Calculated formula: C44.6 H44 Cl1.2 N8 Yb
• Title of publication: Syntheses, characterization and crystal structures of 5,14-dihydro-6,8,15,17-tetramethyldibenzo[b,i][1,4,8,11]tetraazacyclotetradecine rare earth(III) complexes
• Authors of publication: Wang, Zenglin; Hu, Ninghai; Sakata, Kazunori; Hashimoto, Mamoru
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 1999
• Journal issue: 10
• Pages of publication: 1695
• a: 17.143 ± 0.003 Å
• b: 16.135 ± 0.003 Å
• c: 16.239 ± 0.003 Å
• α: 90°
• β: 93.95 ± 0.03°
• γ: 90°
• Cell volume: 4481.1 ± 1.4 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 12
• Hermann-Mauguin space group symbol: C 1 2/m 1
• Hall space group symbol: -C 2y
• Residual factor for all reflections: 0.1035
• Residual factor for significantly intense reflections: 0.0705
• Weighted residual factors for all reflections: 0.2379
• Weighted residual factors for significantly intense reflections: 0.1856
• Goodness-of-fit parameter for all reflections: 1.118
• Goodness-of-fit parameter for significantly intense reflections: 1.254
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No