Information card for entry 7027280

Structure parameters

• Formula: C35 H49 Cl5 Cu N5 Nd O37
• Calculated formula: C35 H49 Cl5 Cu N5 Nd O37
• Title of publication: Synthesis and structures of carboxylate-bridged polynuclear copper(II)‒lanthanide(III) complexes [CuLn(C5H5N+CH2CO2−)5(H2O)5][ClO4]5·2H2O (Ln = La or Nd) and [Cu3Nd2(C5H5N+CH2CO2−)10(NO3)2(H2O)8][ClO4]10·4H2O
• Authors of publication: Yang, Yang-Yi; Wu, Yu-Luan; Long, La-Sheng; Chen, Xiao-Ming
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 1999
• Journal issue: 12
• Pages of publication: 2005
• a: 37.51 ± 0.02 Å
• b: 11.172 ± 0.003 Å
• c: 27.557 ± 0.014 Å
• α: 90°
• β: 104.81 ± 0.01°
• γ: 90°
• Cell volume: 11164 ± 9 ų
• Cell temperature: 294 ± 2 K
• Ambient diffraction temperature: 294 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.116
• Residual factor for significantly intense reflections: 0.0457
• Weighted residual factors for significantly intense reflections: 0.156
• Weighted residual factors for all reflections included in the refinement: 0.1843
• Goodness-of-fit parameter for all reflections included in the refinement: 1.024
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No