Crystallography Open Database

Information card for entry 7027290

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Coordinates	7027290.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C33 H44 B N10 O2 Tc
Calculated formula	C33 H44 B N10 O2 Tc
Title of publication	Technetium(V) and rhenium(V) complexes of biguanide derivatives. Crystal structures
Authors of publication	Marchi, Andrea; Marvelli, Lorenza; Cattabriga, Michela; Rossi, Roberto; Neves, Maria; Bertolasi, Valerio; Ferretti, Valeria
Journal of publication	Journal of the Chemical Society, Dalton Transactions
Year of publication	1999
Journal issue	12
Pages of publication	1937
a	11.589 ± 0.002 Å
b	15.918 ± 0.002 Å
c	18.962 ± 0.004 Å
α	90 ± 0°
β	96.97 ± 0.01°
γ	90 ± 0°
Cell volume	3472.1 ± 1 Å³
Cell temperature	295 K
Ambient diffraction temperature	295 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for significantly intense reflections	0.042
Weighted residual factors for all reflections included in the refinement	0.062
Goodness-of-fit parameter for all reflections included in the refinement	2.23
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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