Crystallography Open Database

Information card for entry 7027298

Preview

Coordinates	7027298.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C27.5 H20 O16 Os6 S4
Calculated formula	C31 H24 O16 Os6 S4
Title of publication	Synthesis, structural characterization and reactivities of hexaosmium carbonyl clusters with six-membered cyclic thioether and thioxane ligands
Authors of publication	Leung, Kelvin Sze-Yin; Wong, Wing-Tak
Journal of publication	Journal of the Chemical Society, Dalton Transactions
Year of publication	1999
Journal issue	12
Pages of publication	2077
a	9.181 ± 0.001 Å
b	28.787 ± 0.001 Å
c	16.533 ± 0.001 Å
α	90°
β	102.38 ± 0.01°
γ	90°
Cell volume	4268 ± 0.6 Å³
Cell temperature	298.2 K
Ambient diffraction temperature	298.2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for significantly intense reflections	0.0651
Weighted residual factors for significantly intense reflections	0.0703
Goodness-of-fit parameter for significantly intense reflections	0.97
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKalpha
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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