Information card for entry 7027302

Structure parameters

• Formula: C23 H18 O17 Os6 S2
• Calculated formula: C23 H18 O17 Os6 S2
• Title of publication: Synthesis, structural characterization and reactivities of hexaosmium carbonyl clusters with six-membered cyclic thioether and thioxane ligands
• Authors of publication: Leung, Kelvin Sze-Yin; Wong, Wing-Tak
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 1999
• Journal issue: 12
• Pages of publication: 2077
• a: 8.992 ± 0.001 Å
• b: 10.348 ± 0.002 Å
• c: 18.637 ± 0.002 Å
• α: 99 ± 0.02°
• β: 94.67 ± 0.01°
• γ: 104.25 ± 0.01°
• Cell volume: 1647 ± 0.4 ų
• Cell temperature: 298.2 K
• Ambient diffraction temperature: 298.2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for significantly intense reflections: 0.0605
• Weighted residual factors for significantly intense reflections: 0.0654
• Goodness-of-fit parameter for significantly intense reflections: 0.979
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKalpha
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No