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Information card for entry 7027315
Preview
Coordinates | 7027315.cif |
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Original paper (by DOI) | HTML |
Formula | C33 H28 Cl O P2 Rh |
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Calculated formula | C33 H28 Cl O P2 Rh |
Title of publication | Binuclear complexes with ligands based on the 2,6-bis(diphenylphosphinomethyl)benzene framework. Syntheses and crystal structures of [Ir2Cl2(μ-CO){2,6-(Ph2PCH2)2C6H3S}2]·2CH2Cl2, [Ni2{2,6-(Ph2PCH2)2C6H4S}2][PF6]2·Et2O·0.5CH2Cl2 and [Rh2Cl2(CO)2{1,3-(Ph2PCH2)2C6H4}2] |
Authors of publication | Dilworth, Jonathan R.; Zheng, Yifan; Vaughan Griffiths, D. |
Journal of publication | Journal of the Chemical Society, Dalton Transactions |
Year of publication | 1999 |
Journal issue | 11 |
Pages of publication | 1877 |
a | 12.094 ± 0.005 Å |
b | 16.45 ± 0.003 Å |
c | 14.604 ± 0.005 Å |
α | 90° |
β | 90.2 ± 0.02° |
γ | 90° |
Cell volume | 2905.4 ± 1.6 Å3 |
Cell temperature | 293 ± 2 K |
Ambient diffraction temperature | 293 ± 2 K |
Number of distinct elements | 6 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/a 1 |
Hall space group symbol | -P 2yab |
Residual factor for all reflections | 0.1729 |
Residual factor for significantly intense reflections | 0.0609 |
Weighted residual factors for all reflections | 0.1934 |
Weighted residual factors for significantly intense reflections | 0.1496 |
Goodness-of-fit parameter for all reflections | 0.957 |
Goodness-of-fit parameter for significantly intense reflections | 1.09 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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