Zirconium mixed ligand isopropoxide/aminoalkoxide complexes: crystal structures of [Zr2(OPri)6(L)2] and [Zr2(OBut)3(bdmap)4(OH)] {where L = dmap, 1-dimethylaminopropan-2-olate and bdmap, 1,1-bis(dimethylamino)propan-2-olate}
Authors of publication
Fleeting, Kirsty A.; O’Brien, Paul; Jones, Anthony C.; Otway, David J.; White, Andrew J. P.; Williams, David J.
Journal of publication
Journal of the Chemical Society, Dalton Transactions
Year of publication
1999
Journal issue
16
Pages of publication
2853
a
12.5887 ± 0.0014 Å
b
14.147 ± 0.002 Å
c
17.0623 ± 0.0013 Å
α
86.483 ± 0.008°
β
70.62 ± 0.008°
γ
85.225 ± 0.011°
Cell volume
2854.7 ± 0.6 Å3
Cell temperature
203 ± 2 K
Ambient diffraction temperature
203 ± 2 K
Number of distinct elements
5
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.1136
Residual factor for significantly intense reflections
0.0561
Weighted residual factors for all reflections
0.1427
Weighted residual factors for significantly intense reflections
0.1136
Goodness-of-fit parameter for all reflections
1.009
Goodness-of-fit parameter for significantly intense reflections
