Information card for entry 7027384

Structure parameters

• Formula: C47 H38 Cl2 N10 Ni2 O8
• Calculated formula: C47 H38 Cl2 N10 Ni2 O8
• Title of publication: Electrochemical synthesis and structural characterisation of transition metal complexes with 2,6-bis(1-salicyloylhydrazonoethyl)pyridine, H4daps
• Authors of publication: Bermejo, Manuel R.; Fondo, Matilde; González, Ana M.; Hoyos, Olga L.; Sousa, Antonio; McAuliffe, Charles A.; Hussain, Wasif; Pritchard, Robin; Novotorsev, Vladimir M.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 1999
• Journal issue: 13
• Pages of publication: 2211
• a: 12.739 ± 0.003 Å
• b: 14.266 ± 0.003 Å
• c: 14.699 ± 0.003 Å
• α: 77 ± 0.03°
• β: 84.61 ± 0.03°
• γ: 63.04 ± 0.03°
• Cell volume: 2319.9 ± 1.1 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0363
• Residual factor for significantly intense reflections: 0.0363
• Weighted residual factors for significantly intense reflections: 0.0971
• Weighted residual factors for all reflections included in the refinement: 0.0971
• Goodness-of-fit parameter for all reflections included in the refinement: 1.062
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No