Information card for entry 7027388

Structure parameters

• Formula: C19 H9 N O11 Os3
• Calculated formula: C19 H9 N O11 Os3
• Title of publication: Orientational isomerism in bridging 2-pyridyl complexes: orthometallation of (S )-nicotine and (R)-1-(4-pyridyl)ethanol in triosmium clusters
• Authors of publication: Deeming, Antony J.; Stchedroff, Marc J.; Whittaker, Caroline; Arce, Alejandro J.; De Sanctis, Ysaura; Steed, Jonathan W.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 1999
• Journal issue: 18
• Pages of publication: 3289
• a: 21.9372 ± 0.0011 Å
• b: 11.7406 ± 0.0008 Å
• c: 9.1656 ± 0.0004 Å
• α: 90°
• β: 93.68 ± 0.003°
• γ: 90°
• Cell volume: 2355.8 ± 0.2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 5
• Hermann-Mauguin space group symbol: C 1 2 1
• Hall space group symbol: C 2y
• Residual factor for all reflections: 0.0414
• Residual factor for significantly intense reflections: 0.0377
• Weighted residual factors for significantly intense reflections: 0.0847
• Weighted residual factors for all reflections included in the refinement: 0.0859
• Goodness-of-fit parameter for all reflections included in the refinement: 1.047
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No