Information card for entry 7027442

Structure parameters

• Formula: C38 H59 O2 Sb
• Calculated formula: C38 H59 O2 Sb
• SMILES: [Sb](C(=O)c1c(cc(cc1C(C)(C)C)C(C)(C)C)C(C)(C)C)=C(O)c1c(cc(cc1C(C)(C)C)C(C)(C)C)C(C)(C)C
• Title of publication: Compounds containing λ3,σ2-SbC bonds: synthesis and structural characterisation of the first stiba-enol, Mes*C(O)SbC(OH)Mes* (Mes* = C6H2But3-2,4,6) and a 2,3-distibabutadiene, {Mes(Me3SiO)CSb}2 (Mes = C6H2Me3-2,4,6) †
• Authors of publication: Jones, Cameron; Steed, Jonathan W.; Thomas, Ryan C.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 1999
• Journal issue: 10
• Pages of publication: 1541
• a: 11.4906 ± 0.0002 Å
• b: 20.0826 ± 0.0004 Å
• c: 31.2742 ± 0.0005 Å
• α: 90°
• β: 90 ± 0.002°
• γ: 90°
• Cell volume: 7216.9 ± 0.2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 4
• Space group number: 61
• Hermann-Mauguin space group symbol: P c a b
• Hall space group symbol: -P 2bc 2ac
• Residual factor for all reflections: 0.0632
• Residual factor for significantly intense reflections: 0.0423
• Weighted residual factors for significantly intense reflections: 0.0833
• Weighted residual factors for all reflections included in the refinement: 0.0894
• Goodness-of-fit parameter for all reflections included in the refinement: 1.079
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No