Information card for entry 7027446

Structure parameters

• Formula: C26 H24 Cl2 Co N4 O4
• Calculated formula: C28 H14 Cl4 Co N4 O4
• Title of publication: Synthesis, crystal structure and properties of trigonal bipyramidal [M(L5)2(H2O)]·H2O complexes [M = cobalt(II) (S = 3/2) or copper(II) (S = 1/2); HL5 = N-(2-chloro-6-methylphenyl)pyridine-2-carboxamide]
• Authors of publication: Patra, Apurba Kumar; Ray, Manabendra; Mukherjee, Rabindranath
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 1999
• Journal issue: 15
• Pages of publication: 2461
• a: 21.039 ± 0.009 Å
• b: 15.841 ± 0.003 Å
• c: 15.678 ± 0.005 Å
• α: 90 ± 0.01°
• β: 90 ± 0.03°
• γ: 90 ± 0.03°
• Cell volume: 5225 ± 3 ų
• Cell temperature: 293 K
• Ambient diffraction temperature: 293 K
• Number of distinct elements: 6
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.149
• Residual factor for significantly intense reflections: 0.058
• Weighted residual factors for all reflections: 0.058
• Weighted residual factors for significantly intense reflections: 0.046
• Goodness-of-fit parameter for all reflections: 1.968
• Goodness-of-fit parameter for significantly intense reflections: 2.499
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoK-alpha
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No