Crystallography Open Database

Information card for entry 7027475

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Coordinates	7027475.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C56 H72 N3 O4 Si Y
Calculated formula	C56 H72 N3 O4 Si Y
Title of publication	Grafting of bulky rare earth metal complexes onto mesoporous silica MCM-41 †
Authors of publication	Anwander, Reiner; Görlitzer, Hans W.; Gerstberger, Gisela; Palm, Clemens; Runte, Oliver; Spiegler, Michael
Journal of publication	Journal of the Chemical Society, Dalton Transactions
Year of publication	1999
Journal issue	20
Pages of publication	3611
a	11.1378 ± 0.0002 Å
b	16.8068 ± 0.0005 Å
c	18.0549 ± 0.0005 Å
α	108.218 ± 0.001°
β	102.675 ± 0.0015°
γ	106.052 ± 0.0016°
Cell volume	2906.8 ± 0.14 Å³
Cell temperature	193 K
Ambient diffraction temperature	193 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0608
Residual factor for significantly intense reflections	0.0522
Weighted residual factors for significantly intense reflections	0.1369
Weighted residual factors for all reflections included in the refinement	0.1433
Goodness-of-fit parameter for all reflections included in the refinement	1.018
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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