Information card for entry 7027583

Structure parameters

• Formula: C63 H66 N2 O6 Si4 W
• Calculated formula: C63 H58 N2 O6 Si4 W
• Title of publication: High oxidation state chromium, molybdenum and tungsten imido metallasiloxanes
• Authors of publication: King, Lawrence; Motevalli, Majid; Sullivan, Alice C.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 1999
• Journal issue: 18
• Pages of publication: 3225
• a: 10.333 ± 0.004 Å
• b: 10.733 ± 0.008 Å
• c: 14.149 ± 0.007 Å
• α: 110.88 ± 0.06°
• β: 90.08 ± 0.04°
• γ: 99.91 ± 0.04°
• Cell volume: 1440.9 ± 1.5 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0696
• Residual factor for significantly intense reflections: 0.0638
• Weighted residual factors for significantly intense reflections: 0.1566
• Weighted residual factors for all reflections included in the refinement: 0.1619
• Goodness-of-fit parameter for all reflections included in the refinement: 1.258
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No