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Information card for entry 7027612
Preview
Coordinates | 7027612.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C31 H25 Cl3 N6 O12 Pt2 S |
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Calculated formula | C31 H25 Cl3 N6 O12 Pt2 S |
SMILES | [Pt]12([S]([Pt]34[n]5ccccc5c5cccc([n]35)c3[n]4cccc3)C)[n]3ccccc3c3cccc([n]13)c1[n]2cccc1.Cl(=O)(=O)(=O)[O-].Cl(=O)(=O)(=O)[O-].Cl(=O)(=O)(=O)[O-] |
Title of publication | Platinum assisted cyclization of S-methyl 3-acyl-2-methyldithiocarbazates under mild conditions. Crystal structure of [Pt2(μ-SMe)(terpy)2][ClO4]3 † |
Authors of publication | Annibale, Giuliano; Bergamini, Paola; Bertolasi, Valerio; Cattabriga, Michela; Lazzaro, Antonio; Marchi, Andrea; Vertuani, Gianni |
Journal of publication | Journal of the Chemical Society, Dalton Transactions |
Year of publication | 1999 |
Journal issue | 21 |
Pages of publication | 3877 |
a | 12.538 ± 0.001 Å |
b | 21.802 ± 0.002 Å |
c | 13.969 ± 0.001 Å |
α | 90° |
β | 106.38 ± 0.01° |
γ | 90° |
Cell volume | 3663.5 ± 0.5 Å3 |
Cell temperature | 293 ± 2 K |
Ambient diffraction temperature | 293 ± 2 K |
Number of distinct elements | 7 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.1131 |
Residual factor for significantly intense reflections | 0.0509 |
Weighted residual factors for significantly intense reflections | 0.1047 |
Weighted residual factors for all reflections included in the refinement | 0.1389 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.124 |
Diffraction radiation wavelength | 0.71069 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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