Information card for entry 7027665

Structure parameters

• Formula: C14 H33 I2 O P2 Rh
• Calculated formula: C14 H33 I2 O P2 Rh
• Title of publication: The carbonylation of methanol catalysed by [RhI(CO)(PEt3)2]; crystal and molecular structure of [RhMeI2(CO)(PEt3)2] †
• Authors of publication: Rankin, Joanne; Benyei, Attila C.; Poole, Andrew D.; Cole-Hamilton, David J.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 1999
• Journal issue: 21
• Pages of publication: 3771
• a: 7.402 ± 0.005 Å
• b: 11.785 ± 0.005 Å
• c: 12.52 ± 0.004 Å
• α: 90°
• β: 96.01 ± 0.04°
• γ: 90°
• Cell volume: 1086.1 ± 0.9 ų
• Cell temperature: 493.2 K
• Ambient diffraction temperature: 493.2 K
• Number of distinct elements: 6
• Space group number: 7
• Hermann-Mauguin space group symbol: P 1 n 1
• Hall space group symbol: P -2yac
• Residual factor for significantly intense reflections: 0.0263
• Weighted residual factors for significantly intense reflections: 0.0272
• Goodness-of-fit parameter for significantly intense reflections: 4.042
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKalpha
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No