Information card for entry 7027669

Structure parameters

• Formula: C19 H25 Co1.5 N2 O11
• Calculated formula: C19 H13 Co1.5 N2 O11
• Title of publication: Crystallisation of H3BTC, H3TPO or H2SDA with MII (M = Co, Mn or Zn) and 2,2′-bipyridyl: design and control of co-ordination architecture, and magnetic properties (H3BTC = benzene-1,3,5-tricarboxylic acid, H3TPO = tris(4-carboxylphenyl)phosphine oxide, H2SDA = cis-stilbene-4,4′-dicarboxylic acid) †
• Authors of publication: Plater, M. John; Foreman, Mark R. St. J.; Coronado, Eugenio; Gómez-García, Carlos J.; Slawin, Alexandra M. Z.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 1999
• Journal issue: 23
• Pages of publication: 4209
• a: 10.0443 ± 0.0007 Å
• b: 10.3414 ± 0.0007 Å
• c: 12.1092 ± 0.0009 Å
• α: 74.719 ± 0.002°
• β: 74.947 ± 0.002°
• γ: 79.909 ± 0.002°
• Cell volume: 1163.98 ± 0.14 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1405
• Residual factor for significantly intense reflections: 0.0482
• Weighted residual factors for all reflections: 0.1437
• Weighted residual factors for significantly intense reflections: 0.0938
• Goodness-of-fit parameter for all reflections: 0.571
• Goodness-of-fit parameter for significantly intense reflections: 0.879
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No