Information card for entry 7027682

Structure parameters

• Formula: C61 H60 Cl2 O4 P4 Ru
• Calculated formula: C61 H60 Cl2 O4 P4 Ru
• Title of publication: Bis(acetylacetonato)bis(cyclooctene)ruthenium(II), cis-[Ru(acac)2(η2-C8H14)2]: a synthetic precursor to trans- and cis-bis(acetylacetonato)ruthenium(II) complexes †
• Authors of publication: Bennett, Martin A.; Chung, Guandolina; Hockless, David C. R.; Neumann, Horst; Willis, Anthony C.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 1999
• Journal issue: 19
• Pages of publication: 3451
• a: 10.774 ± 0.002 Å
• b: 11.362 ± 0.003 Å
• c: 13.463 ± 0.003 Å
• α: 66.78 ± 0.02°
• β: 74.2 ± 0.01°
• γ: 86.95 ± 0.02°
• Cell volume: 1454.6 ± 0.6 ų
• Cell temperature: 296.2 K
• Ambient diffraction temperature: 296.2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0765
• Residual factor for significantly intense reflections: 0.0378
• Weighted residual factors for all reflections: 0.0411
• Weighted residual factors for all reflections included in the refinement: 0.0371
• Goodness-of-fit parameter for all reflections: 1.459
• Goodness-of-fit parameter for all reflections included in the refinement: 1.62
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No