Information card for entry 7027703

Structure parameters

• Formula: C21 H15 As Mo O6 W2
• Calculated formula: C21 As Mo1.005 O6 W2.005
• Title of publication: Synthesis, reactivity and structural characterization of some heterometallic complexes containing naked arsenic ligands †
• Authors of publication: Adams, Katherine V.; Choi, Nick; Conole, Gráinne; Davies, John E.; King, Jason D.; Mays, Martin J.; McPartlin, Mary; Raithby, Paul R.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 1999
• Journal issue: 21
• Pages of publication: 3679
• a: 14.042 ± 0.002 Å
• b: 7.513 ± 0.0015 Å
• c: 20.877 ± 0.004 Å
• α: 90°
• β: 91.762 ± 0.009°
• γ: 90°
• Cell volume: 2201.4 ± 0.7 ų
• Cell temperature: 295 ± 2 K
• Ambient diffraction temperature: 295 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0949
• Residual factor for significantly intense reflections: 0.0625
• Weighted residual factors for significantly intense reflections: 0.1595
• Weighted residual factors for all reflections included in the refinement: 0.1803
• Goodness-of-fit parameter for all reflections included in the refinement: 1.049
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No