Information card for entry 7027730

Structure parameters

• Formula: C24 H27 Cl3 N2 O10 Re
• Calculated formula: C24 H24 Cl3 N2 O10 Re
• Title of publication: A luminescent tricarbonylchlororhenium(I) complex featuring a flexible “crown ether” ligand. Manipulation of photoexcited state properties via binding of small cations †
• Authors of publication: Bélanger, Suzanne; Gilbertson, Michelle; Yoon, Dong I.; Stern, Charlotte L.; Dang, Xiaojun; Hupp, Joseph T.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 1999
• Journal issue: 19
• Pages of publication: 3407
• a: 10.312 ± 0.003 Å
• b: 12.391 ± 0.002 Å
• c: 13.02 ± 0.003 Å
• α: 63.94 ± 0.01°
• β: 84.54 ± 0.02°
• γ: 80.56 ± 0.02°
• Cell volume: 1473.8 ± 0.6 ų
• Cell temperature: 153 ± 2 K
• Ambient diffraction temperature: 153 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1203
• Weighted residual factors for all reflections: 0.1269
• Goodness-of-fit parameter for all reflections: 1.804
• Goodness-of-fit parameter for significantly intense reflections: 1.804
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No