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Information card for entry 7027746
Preview
Coordinates | 7027746.cif |
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Original paper (by DOI) | HTML |
Formula | C24 H26 Cl2 N3 P Pd S |
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Calculated formula | C24 H26 Cl2 N3 P Pd S |
Title of publication | Formation, characterization, and structural studies of novel thiosemicarbazone palladium(II) complexes. Crystal structures of [{Pd[C6H4C(Et)NNC(S)NH2]}4], [Pd{C6H4C(Et)NN C(S)NH2}(PMePh2)] and [{Pd[C6H4C(Et)NNC(S)NH2]}2(μ-Ph2PCH2PPh2)] |
Authors of publication | Vila, José M.; Pereira, Ma Teresa; Ortigueira, Juan M.; Graña, María; Lata, Darío; Suárez, Antonio; Fernández, Jesús J.; Fernández, Alberto; López-Torres, Margarita; Adams, Harry |
Journal of publication | Journal of the Chemical Society, Dalton Transactions |
Year of publication | 1999 |
Journal issue | 23 |
Pages of publication | 4193 |
a | 15.366 ± 0.003 Å |
b | 9.174 ± 0.002 Å |
c | 18.525 ± 0.003 Å |
α | 90° |
β | 104.2 ± 0.02° |
γ | 90° |
Cell volume | 2531.6 ± 0.9 Å3 |
Cell temperature | 293 ± 2 K |
Ambient diffraction temperature | 293 ± 2 K |
Number of distinct elements | 7 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.0587 |
Residual factor for significantly intense reflections | 0.05 |
Weighted residual factors for all reflections | 0.1468 |
Weighted residual factors for significantly intense reflections | 0.1393 |
Goodness-of-fit parameter for all reflections | 1.15 |
Goodness-of-fit parameter for significantly intense reflections | 1.189 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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