Crystallography Open Database

Information card for entry 7027792

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Coordinates	7027792.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C16 H28 B2 N4
Calculated formula	C16 H28 B2 N4
Title of publication	Synthesis and characterization of new azido(o-phenylenedioxy)boranes and azidobicyclononylboranes †
Authors of publication	Fraenk, Wolfgang; Habereder, Tassilo; Klapötke, Thomas M.; Nöth, Heinrich; Polborn, Kurt
Journal of publication	Journal of the Chemical Society, Dalton Transactions
Year of publication	1999
Journal issue	23
Pages of publication	4283
a	24.819 ± 0.006 Å
b	7.4217 ± 0.0014 Å
c	19.099 ± 0.003 Å
α	90 ± 0.013°
β	106.29 ± 0.02°
γ	90 ± 0.02°
Cell volume	3376.8 ± 1.2 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	4
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0776
Residual factor for significantly intense reflections	0.0559
Weighted residual factors for all reflections	0.1493
Weighted residual factors for significantly intense reflections	0.1319
Goodness-of-fit parameter for all reflections	1.084
Goodness-of-fit parameter for significantly intense reflections	1.128
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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