Information card for entry 7027795

Structure parameters

• Formula: C62.5 H73 B2 Cl13 Mo2 N16 O3
• Calculated formula: C62.5 H62 B2 Cl13 Mo2 N16 O3
• Title of publication: Complexes containing redox-active fluorenone-based ligands linked to redox-active tris(pyrazolyl)boratomolybdenum fragments: assignment of ligand-centred and metal-centred redox processes by EPR and UV/VIS/NIR spectroelectrochemistry †
• Authors of publication: Behrendt, Andreas; Couchman, Samantha M.; Jeffery, John C.; McCleverty, Jon A.; Ward, Michael D.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 1999
• Journal issue: 24
• Pages of publication: 4349
• a: 9.401 ± 0.002 Å
• b: 17.73 ± 0.004 Å
• c: 25.841 ± 0.007 Å
• α: 105.48 ± 0.02°
• β: 93.23 ± 0.02°
• γ: 100.63 ± 0.02°
• Cell volume: 4054.3 ± 1.8 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.2395
• Residual factor for significantly intense reflections: 0.1048
• Weighted residual factors for all reflections: 0.3201
• Weighted residual factors for significantly intense reflections: 0.2433
• Goodness-of-fit parameter for all reflections: 1.002
• Goodness-of-fit parameter for significantly intense reflections: 1.251
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No