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Information card for entry 7027795
Preview
Coordinates | 7027795.cif |
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Original paper (by DOI) | HTML |
Formula | C62.5 H73 B2 Cl13 Mo2 N16 O3 |
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Calculated formula | C62.5 H62 B2 Cl13 Mo2 N16 O3 |
Title of publication | Complexes containing redox-active fluorenone-based ligands linked to redox-active tris(pyrazolyl)boratomolybdenum fragments: assignment of ligand-centred and metal-centred redox processes by EPR and UV/VIS/NIR spectroelectrochemistry † |
Authors of publication | Behrendt, Andreas; Couchman, Samantha M.; Jeffery, John C.; McCleverty, Jon A.; Ward, Michael D. |
Journal of publication | Journal of the Chemical Society, Dalton Transactions |
Year of publication | 1999 |
Journal issue | 24 |
Pages of publication | 4349 |
a | 9.401 ± 0.002 Å |
b | 17.73 ± 0.004 Å |
c | 25.841 ± 0.007 Å |
α | 105.48 ± 0.02° |
β | 93.23 ± 0.02° |
γ | 100.63 ± 0.02° |
Cell volume | 4054.3 ± 1.8 Å3 |
Cell temperature | 173 ± 2 K |
Ambient diffraction temperature | 173 ± 2 K |
Number of distinct elements | 7 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.2395 |
Residual factor for significantly intense reflections | 0.1048 |
Weighted residual factors for all reflections | 0.3201 |
Weighted residual factors for significantly intense reflections | 0.2433 |
Goodness-of-fit parameter for all reflections | 1.002 |
Goodness-of-fit parameter for significantly intense reflections | 1.251 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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