Information card for entry 7027821

Structure parameters

• Formula: C18 H30 Mn O3 P5
• Calculated formula: C18 H30 Mn O3 P5
• Title of publication: Synthesis and characterization of pentakis(dimethylphosphanyl)cymantrene [Mn{C5(PMe2)5}(CO)3], the first cyclopentadienyl complex with five phosphanyl substituents †
• Authors of publication: Sünkel, Karlheinz; Stramm, Cornelia; Soheili, Sabine
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 1999
• Journal issue: 24
• Pages of publication: 4299
• a: 10.519 ± 0.002 Å
• b: 14.653 ± 0.003 Å
• c: 17.505 ± 0.004 Å
• α: 72.72 ± 0.02°
• β: 89.84 ± 0.02°
• γ: 79.68 ± 0.02°
• Cell volume: 2531 ± 1 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0842
• Residual factor for significantly intense reflections: 0.0541
• Weighted residual factors for significantly intense reflections: 0.1299
• Weighted residual factors for all reflections included in the refinement: 0.1476
• Goodness-of-fit parameter for all reflections included in the refinement: 1.012
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No