Information card for entry 7027826

Structure parameters

• Common name: [(salen)VOV(O)(salen)][I3]
• Formula: C18 H18 I1.5 N2 O3 V
• Calculated formula: C18 H18 I1.5 N2 O3 V
• Title of publication: New compounds of tetradentate Schiff bases with vanadium(IV) and vanadium(V) †
• Authors of publication: Choudhary, Nosheen F.; Connelly, Neil G.; Hitchcock, Peter B.; Leigh, G. Jeffery
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 1999
• Journal issue: 24
• Pages of publication: 4437
• a: 7.625 ± 0.003 Å
• b: 17.769 ± 0.005 Å
• c: 14.628 ± 0.007 Å
• α: 90°
• β: 93.51 ± 0.04°
• γ: 90°
• Cell volume: 1978.2 ± 1.3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.0842
• Residual factor for significantly intense reflections: 0.0511
• Weighted residual factors for all reflections: 0.1086
• Weighted residual factors for significantly intense reflections: 0.0948
• Goodness-of-fit parameter for all reflections: 1.055
• Goodness-of-fit parameter for significantly intense reflections: 1.138
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No