Information card for entry 7027834

Structure parameters

• Formula: C35 H25 O11 P Ru4 W
• Calculated formula: C35 H25 O11 P Ru4 W
• Title of publication: Synthesis and skeletal isomerization of the phosphinidene acetylide cluster complexes [Ru4(CO)10(μ4-PPh)(CCPh){WL(CO)}] where L = C5Me5 or C5H5
• Authors of publication: Tseng, Wen-Cheng; Chi, Yun; Su, Chi-Jung; Carty, Arthur J.; Peng, Shie-Ming; Lee, Gene-Hsiang
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 1998
• Journal issue: 6
• Pages of publication: 1053
• a: 32.487 ± 0.004 Å
• b: 10.295 ± 0.003 Å
• c: 22.6243 ± 0.0024 Å
• α: 90°
• β: 96.057 ± 0.01°
• γ: 90°
• Cell volume: 7525 ± 3 ų
• Cell temperature: 293 K
• Ambient diffraction temperature: 293 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.052
• Residual factor for significantly intense reflections: 0.027
• Weighted residual factors for all reflections: 0.026
• Weighted residual factors for significantly intense reflections: 0.024
• Goodness-of-fit parameter for significantly intense reflections: 1.32
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MolybdenumKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No