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Information card for entry 7027842
Preview
Coordinates | 7027842.cif |
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Original paper (by DOI) | HTML |
Formula | C48.5 H44 Au N2 O3 P4 S |
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Calculated formula | C48.5 H41 Au N2 O3 P4 S |
Title of publication | Synthesis and characterisation of the first E-unidentate [Ph2P(O)NP(E)Ph2]− metal complexes [Au{Ph2P(O)NP(E)Ph2-E }{Ph2P(O)NHPPh2}] and [Pd{Ph2P(O)NP(E)Ph2-E }2(H2NCH2CH2NH2)] (E = S or Se) |
Authors of publication | Slawin, Alexandra M. Z.; Smith, Martin B.; Woollins, J. Derek |
Journal of publication | Journal of the Chemical Society, Dalton Transactions |
Year of publication | 1998 |
Journal issue | 10 |
Pages of publication | 1537 |
a | 39.3439 ± 0.001 Å |
b | 13.2267 ± 0.0003 Å |
c | 18.4912 ± 0.0005 Å |
α | 90° |
β | 91.473 ± 0.001° |
γ | 90° |
Cell volume | 9619.5 ± 0.4 Å3 |
Cell temperature | 293 ± 2 K |
Ambient diffraction temperature | 293 ± 2 K |
Number of distinct elements | 7 |
Space group number | 15 |
Hermann-Mauguin space group symbol | C 1 2/c 1 |
Hall space group symbol | -C 2yc |
Residual factor for all reflections | 0.1136 |
Residual factor for significantly intense reflections | 0.0496 |
Weighted residual factors for all reflections | 2.5373 |
Weighted residual factors for significantly intense reflections | 0.1074 |
Goodness-of-fit parameter for all reflections | 0.403 |
Goodness-of-fit parameter for significantly intense reflections | 0.755 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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