Information card for entry 7027855

Structure parameters

• Formula: C33 H74 B26 P3 Pt2
• Calculated formula: C33 H61 B26 P3 Pt2
• Title of publication: Macropolyhedral boron-containing cluster chemistry. Mixed and multiple cluster fusion in platinaborane chemistry and the structure of [(PMe2Ph)2PtB16H17PtB10H11(PMe2Ph)] as determined by synchrotron X-ray diffraction analysis
• Authors of publication: Bould, Jonathan; Clegg, William; Kennedy, John D.; Teat, Simon J.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 1998
• Journal issue: 17
• Pages of publication: 2777
• a: 14.7903 ± 0.0004 Å
• b: 13.0595 ± 0.0003 Å
• c: 28.3431 ± 0.0007 Å
• α: 90°
• β: 90.452 ± 0.002°
• γ: 90°
• Cell volume: 5474.4 ± 0.2 ų
• Cell temperature: 160 ± 2 K
• Ambient diffraction temperature: 160 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0548
• Residual factor for significantly intense reflections: 0.0375
• Weighted residual factors for significantly intense reflections: 0.0799
• Weighted residual factors for all reflections included in the refinement: 0.0861
• Goodness-of-fit parameter for all reflections included in the refinement: 1.087
• Diffraction radiation wavelength: 0.6874 Å
• Diffraction radiation type: synchrotron
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No