Information card for entry 7028029

Structure parameters

• Formula: C43 H38 N3 O P2 Re
• Calculated formula: C43 H38 N3 O P2 Re
• Title of publication: Syntheses and structural characterizations of phenylimidorhenium(V) complexes containing bi- or tetra-dentate phosphinoamido ligands
• Authors of publication: Refosco, Fiorenzo; Bolzati, Cristina; Tisato, Francesco; Bandoli, Giuliano
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 1998
• Journal issue: 6
• Pages of publication: 923
• a: 11.816 ± 0.004 Å
• b: 21.028 ± 0.007 Å
• c: 15.085 ± 0.004 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 3748 ± 2 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 62
• Hermann-Mauguin space group symbol: P n m a
• Hall space group symbol: -P 2ac 2n
• Residual factor for all reflections: 0.0655
• Residual factor for significantly intense reflections: 0.0484
• Weighted residual factors for all reflections: 0.3022
• Weighted residual factors for significantly intense reflections: 0.1299
• Goodness-of-fit parameter for all reflections: 1.186
• Goodness-of-fit parameter for significantly intense reflections: 1.259
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No