Information card for entry 7028061

Structure parameters

• Chemical name: μ-ethane-1,2-diyl-bis[bis(dimethylglyoximato-N,N')(triphenylphos phine) rhodium(III)]
• Formula: C54 H62 N8 O8 P2 Rh2
• Calculated formula: C54 H62 N8 O8 P2 Rh2
• Title of publication: Syntheses and structures of novel cyclic and dinuclear organorhodoximes: a homologous series of di- to penta-methylene-bridged complexes ‡
• Authors of publication: Steinborn, Dirk; Rausch, Mario; Bruhn, Clemens; Schmidt, Harry; Ströhl, Dieter
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 1998
• Journal issue: 2
• Pages of publication: 221
• a: 16.5199 ± 0.0015 Å
• b: 9.931 ± 0.002 Å
• c: 16.721 ± 0.003 Å
• α: 90°
• β: 100.278 ± 0.011°
• γ: 90°
• Cell volume: 2699.2 ± 0.8 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0515
• Residual factor for significantly intense reflections: 0.0318
• Weighted residual factors for all reflections: 0.0836
• Weighted residual factors for significantly intense reflections: 0.0718
• Goodness-of-fit parameter for all reflections: 1.111
• Goodness-of-fit parameter for significantly intense reflections: 1.102
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No