Information card for entry 7028064

Structure parameters

• Formula: C29 H34 N4 O4 P Rh
• Calculated formula: C29 H34 N4 O4 P Rh
• SMILES: [Rh]123(CCCO[N]1=C(C(C)=N2=O)C)([N](=C(C(C)=N3=O)C)O)[P](c1ccccc1)(c1ccccc1)c1ccccc1
• Title of publication: Syntheses and structures of novel cyclic and dinuclear organorhodoximes: a homologous series of di- to penta-methylene-bridged complexes ‡
• Authors of publication: Steinborn, Dirk; Rausch, Mario; Bruhn, Clemens; Schmidt, Harry; Ströhl, Dieter
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 1998
• Journal issue: 2
• Pages of publication: 221
• a: 15.298 ± 0.002 Å
• b: 11.928 ± 0.002 Å
• c: 33.903 ± 0.005 Å
• α: 90°
• β: 100.232 ± 0.012°
• γ: 90°
• Cell volume: 6088 ± 1.6 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: I 1 2/a 1
• Hall space group symbol: -I 2ya
• Residual factor for all reflections: 0.0956
• Residual factor for significantly intense reflections: 0.0649
• Weighted residual factors for all reflections: 0.2269
• Weighted residual factors for significantly intense reflections: 0.2063
• Goodness-of-fit parameter for all reflections: 1.116
• Goodness-of-fit parameter for significantly intense reflections: 1.206
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No