Information card for entry 7028130

Structure parameters

• Formula: C36 H48 N4 O4 Os
• Calculated formula: C37 H49 N4 O4 Os
• Title of publication: Nitrido-ruthenium(VI) and -osmium(VI) complexes containing chelating multianionic (N, O) ligands. Synthesis, crystal structures and reactions with triphenylphosphine
• Authors of publication: Chan, Pui-Ming; Yu, Wing-Yiu; Che, Chi-Ming; Cheung, Kung-Kai
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 1998
• Journal issue: 19
• Pages of publication: 3183
• a: 19.816 ± 0.002 Å
• b: 22.746 ± 0.004 Å
• c: 15.43 ± 0.002 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 6954.8 ± 1.7 ų
• Cell temperature: 301.2 K
• Ambient diffraction temperature: 301.2 K
• Number of distinct elements: 5
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for significantly intense reflections: 0.0315
• Weighted residual factors for significantly intense reflections: 0.0409
• Goodness-of-fit parameter for significantly intense reflections: 1.289
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKalpha
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No