Information card for entry 7028151

Structure parameters

• Formula: C66.5 H70 Ag3 B2 Cl N12 O12
• Calculated formula: C66.5 H69 Ag3 B2 Cl N12 O12
• Title of publication: An unprecedented trinucleating bridging mode (μ3-η1∶η1∶η1) of a tris(pyrazolyl)borate ligand in a trinuclear silver(I) complex
• Authors of publication: Humphrey, Elizabeth R.; Harden, Nicholas C.; Rees, Leigh H.; Jeffery, John C.; McCleverty, Jon A.; Ward, Michael D.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 1998
• Journal issue: 20
• Pages of publication: 3353
• a: 15.264 ± 0.004 Å
• b: 15.785 ± 0.004 Å
• c: 29.433 ± 0.011 Å
• α: 90°
• β: 103.853 ± 0.015°
• γ: 90°
• Cell volume: 6885 ± 4 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.078
• Residual factor for significantly intense reflections: 0.0426
• Weighted residual factors for all reflections: 0.0986
• Weighted residual factors for significantly intense reflections: 0.0865
• Goodness-of-fit parameter for all reflections: 1
• Goodness-of-fit parameter for significantly intense reflections: 1.071
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No