Information card for entry 7028160

Structure parameters

• Chemical name: Bis(2,9-dimethyl-1-10-phenanthroline)Copper(I) Tetrafluoroborate dichloromethane solvate (2:1)
• Formula: C28.5 H25 B Cl Cu F4 N4
• Calculated formula: C28.5 H24 B Cl Cu F4 N4
• Title of publication: Copper(I) chelated by 2,9-dimethyl-1,10-phenanthroline and bridged by 4,4′-bipyridine or trans-1,2-bis(pyridin-4-yl)ethene to give discrete dinuclear and polymeric cations
• Authors of publication: Blake, Alexander J.; Hill, Stuart J.; Hubberstey, Peter; Li, Wan-Sheung
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 1998
• Journal issue: 6
• Pages of publication: 909
• a: 10.514 ± 0.002 Å
• b: 11.119 ± 0.002 Å
• c: 12.889 ± 0.002 Å
• α: 67.27 ± 0.02°
• β: 74 ± 0.02°
• γ: 73.17 ± 0.02°
• Cell volume: 1307.2 ± 0.5 ų
• Cell temperature: 150 ± 1 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0645
• Residual factor for significantly intense reflections: 0.0566
• Weighted residual factors for all reflections: 0.0695
• Weighted residual factors for significantly intense reflections: 0.0646
• Goodness-of-fit parameter for all reflections: 1.1329
• Goodness-of-fit parameter for significantly intense reflections: 1.1329
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No