Information card for entry 7028196

Structure parameters

• Chemical name: Potassium {3,5-bis-(2'-hydroxyiminopropanoyl)-1,3,5-oxadiazinane (3-)}nickolate(II) sesquihydrate
• Formula: C9 H16 K N6 Ni O6.5
• Calculated formula: C9 H14.5 K N6 Ni O6.5
• Title of publication: Template synthesis of square-planar nickel(II) and copper(III) complexes based on hydrazide ligands
• Authors of publication: Fritsky, Igor O.; Kozłowski, Henryk; Sadler, Peter J.; Yefetova, Oksana P.; Śwątek-Kozłowska, Jolanta; Kalibabchuk, Valentina A.; Głowiak, Tadeusz
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 1998
• Journal issue: 19
• Pages of publication: 3269
• a: 8.089 ± 0.001 Å
• b: 10.376 ± 0.004 Å
• c: 10.64 ± 0.001 Å
• α: 99.51 ± 0.04°
• β: 111.95 ± 0.02°
• γ: 106.86 ± 0.02°
• Cell volume: 754.1 ± 0.4 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0532
• Residual factor for significantly intense reflections: 0.0425
• Weighted residual factors for all reflections: 0.1066
• Weighted residual factors for significantly intense reflections: 0.0977
• Goodness-of-fit parameter for all reflections: 1.013
• Goodness-of-fit parameter for significantly intense reflections: 1.15
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No