Information card for entry 7028407

Structure parameters

• Formula: C74 H64 Cl4 F2 N2 O10 P7 V
• Calculated formula: C74 H64 Cl4 F2 N2 O10 P7 V
• Title of publication: Facile synthesis of mononuclear early transition-metal complexes of κ3cyclo-tetrametaphosphate ([P4O12]4-) and cyclo-trimetaphosphate ([P3O9]3-.
• Authors of publication: Manna, Cesar M.; Nassar, Mostafa Y.; Tofan, Daniel; Chakarawet, Khetpakorn; Cummins, Christopher C.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2014
• Journal volume: 43
• Journal issue: 4
• Pages of publication: 1509 - 1518
• a: 10.7925 ± 0.0012 Å
• b: 13.5617 ± 0.0014 Å
• c: 24.724 ± 0.003 Å
• α: 83.503 ± 0.002°
• β: 84.906 ± 0.002°
• γ: 88.089 ± 0.002°
• Cell volume: 3580.3 ± 0.7 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0592
• Residual factor for significantly intense reflections: 0.0479
• Weighted residual factors for significantly intense reflections: 0.1261
• Weighted residual factors for all reflections included in the refinement: 0.1344
• Goodness-of-fit parameter for all reflections included in the refinement: 1.029
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No