Information card for entry 7028791

Structure parameters

• Formula: C39 H44 N3 O4 P2
• Calculated formula: C39 H44 N3 O4 P2
• Title of publication: A cascade reaction: ring-opening insertion of dioxaphospholane into lutetium alkyl bonds.
• Authors of publication: Johnson, Kevin R. D.; Hayes, Paul G.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2014
• Journal volume: 43
• Journal issue: 6
• Pages of publication: 2448 - 2457
• a: 10.3386 ± 0.0007 Å
• b: 20.4403 ± 0.0013 Å
• c: 32.986 ± 0.002 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 6970.7 ± 0.8 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.0475
• Residual factor for significantly intense reflections: 0.0382
• Weighted residual factors for significantly intense reflections: 0.0986
• Weighted residual factors for all reflections included in the refinement: 0.1054
• Goodness-of-fit parameter for all reflections included in the refinement: 1.053
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No